تحضير ودراسة فاعلية بعض المركبات الاميدية الجديدة
Asma Omar jebril (1-2012)

The thermovoltaic detection (TVD) technique is based on measurement of the EMF generated by two dissimilar metal electrodes in contact with the specimen. This technique has recently been applied when investigating different types of materials involving thermal decomposition reactions which have more normally been studied by conventional thermal analysis techniques, such as DTA, TG, etc. This paper reports the application of the combined TVD and DTA techniques for thermal characterization of materials. The Harrop DTA system has been modified such that measurements by the two techniques can be made simultaneously in the same environment. Data have been obtained on different types of materials, e.g., NiSO,.6H,O and CoSO,.7H,O, etc., at a programmed heating rate of 10” C rnin- ‘. Results obtained by these techniques are discussed and compared with the corresponding values in the literature.
Ragiab Ali Mokhtar(5-1990)

Salvia officinalis L. is a Mediterranean species, naturalized in many countries. The composition of essential oil isolated from Salvia officinalis L, wild growing in Libya, was analyzed. In this study, essential oils from fresh and dry leaves of Salvia officinalis L, Libya, were extracted with ethanol, hexane or chloroform as solvents using Soxhlet apparatus and the extracts were analyzed using gas chromatography/mass spectrometry method. Each solvent showed differences in the extraction yields between fresh and dry leaves. Physical constants of the extracts were shown variation in color, viscosity, density, PH and percentage of production between fresh and dry leaves for each solvent. GC-MS results showed that ethanol could extract the most compounds compared to hexane and chloroform from both fresh and dry leaves. In total 41, 28 and 31 compounds were identified in the essential oils of fresh and dry leaves of Salvia officinalis L using ethanol, hexane or chloroform respectively. For each solvent the number of compounds extracted from dry leaves was bigger than the number extracted from fresh leaves. arabic 33 English 104
ABUBAKER A BASHIR ATRROG, abdunnaser mohamed mohamed megrahi, Fathia Mousa H Altalhi(4-2018)